Lab Facilities

 

Perkin Elmer TGA - STA 6000 

Thermogravimetric analysis (TGA) is a widely employed technique for measuring the change in weight of a sample as a function of temperature or time in a controlled atmosphere. TGA is reliable equipment for the kinetic studies. The DSC signal measures endothermic and exothermic transitions (e.g. polymorphism, melting, crystallization, etc.) of biomass. - This instrument has simultaneous analysis of TG with DTA mode (dT) and DSC (mW) mode for fast enhanced result interpretation - Operating temperature is 15 to 1000oC, and heating rate is 0.1 to 100oC/min

 

 

High Pressure TGA - Thermax 500

The TherMax 500 system specializes in demanding applications where high temperatures, pressures, and aggressive atmospheres are required. Pressure can be used to enhance or speed up reactions.

The TherMax 500 Pressure TGA can measure samples in a controlled environment. Pressures up to 100 bar and temperatures up to 1000 °C are not a problem, even in an aggressive atmosphere. The system incorporates a pressure control system consisting of mass flow controllers for three gases, back pressure regulator, pressure transducer, flow switches and solenoid valves. The 38mm diameter reactor tube and the high mass balance guarantee the capability of not only high weight measurements, but high volume as well.

  • 100 grams sample capacity
  • 35 mL sample volume, and under various reaction environments, including corrosive and flammable gases.
  • From 10-4 torr to 100 bar.

 

 

 

Micromeritics ASAP 2020 

 

The ASAP 2020 Accelerated Surface Area and Porosimetry Analyzer uses gas sorption techniques for research and quality control applications. Also available is the Chemical Adsorption (Chemisorption) option, which uses the static volumetric technique to determine the percent metal dispersion, active metal surface area, size of active particles, and surface acidity of catalyst materials.

 

 

 

 

 

 

 

Perkin Elmer 2400 Series II CHNS/O

Elemental Analyzer is a powerful instrument for the rapid determination of Carbon, hydrogen, nitrogen, oxygen, sulfur or oxygen content in organic and other type of materials. This single instrument is able to analyze three different modes of operation such as CHN, CHNS and Oxygen.

The 2400 Series II CHNS/O Elemental Analyzer is capable of operating in three modes: CHN, CHNS and Oxygen, is fully automated, and includes a 60 position autosampler. In addition to the instument's "tried and true" design features, the 2400 Series II CHNS/O System includes our intuitive, easy-to-use, EA Data Manager Software. The EA Data Manager software adds powerful capabilities that assist in streamlining your data collection and analyses.

 

 

 

TGA Analyzer (TG-209 F1 Libra)

Thermogravimetric analysis (TGA) is a widely employed technique for measuring the change in weight of a sample as a function of temperature or time in a controlled atmosphere. TGA is reliable equipment for the kinetic studies. This instrument has simultaneous analysis of TG with DTA mode (dT) and DSC (mW) mode.

 

 

 

 

 

TGA-FTIR (PE TGA8000 and Septrum 2 FTIR)

A sample is heated in the TGA, whereby, it decomposes and releases volatile materials and/or gaseous components. TGA provides quantitative information but does not provide information on what the decomposition products are concurrent to the weight loss. Because of its ability to detect functional groups in gas-phase, IR analysis allows greater understanding of the processes seen in the TGA. These gases Thermogravimetric properties are recorded and are then transferred to the IR cell via a high-fidelity transfer system where the components can be further characterized/identified.

 

 

 

ChemBET Pulsar

ChemBET Pulsar combines affordability and automation in a compact benchtop catalyst characterization unit. Programmable analysis sequences combined with an automatic loop injector, gas switching, and furnace temperature ramping enable easy pulse titration and temperature-programmed analyses with minimal user intervention. An advanced data reduction package including peak deconvolution, comparable to high-end catalyst characterization units, comes as a standard.

The standard capabilities of the ChemBET Pulsar are: 

Temperature Programmed Desorption (TPD),Temperature Programmed Reduction (TPR),Temperature Programmed Oxidation (TPO),Temperature Programmed Reaction (TPRx), Catalyst Treatment, Flow BET Surface Area, Pulse Titration, Pulse Calibration

 

 

 

Perkin Elmer Clarus 400

Gas chromatography - specifically gas-liquid chromatography - involves a sample being vaporized and injected onto the head of the chromatographic column. The sample is transported through the column by the flow of inert, gaseous mobile phase. The column itself contains a liquid stationary phase which is adsorbed onto the surface of an inert solid. GC is used in separating and analyzing compounds that can be vaporized without decomposition.

 

 

 

 

 

 

 

HP 6890 GC-MS

GC-MS is an instrument that separates all the compounds in a sample, and analyzes the compounds one by one by generating a mass spectrum. This mass spectrum is a fingerprint that allows us to identify the compounds. This equipment is used to analyze the by-product of the pyrolysis/gasification technique.

 

 

 

 

 

Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES)

This ICP-OES is an analytical technique used for the detection of chemical elements in liquid and solid samples. Agilent’s 5110 Vertical Dual View (VDV) ICP-OES combines speed and analytical performance, so you do not have to compromise on either. The equipment is equipped with a dual view capability (axial and radial view) to enable the quantification of a wide range of elements. The instrument is capable of handling aqueous, organic, and HF matrices. A microwave digestor (MultiWave 5000) is available for the fast digestion of different samples.

 

 

 

Microwave Synthesis/Digestion System (Multiwave 5000)

The Multiwave 5000 is a microwave reaction system for the digestion of samples, evaporation, acid leaching, and extractions. The instrument is used microwave-assisted acid digestion and leaching, extraction, synthesis, and hydrolysis. It has an easy-to-navigate user interface with more than 500 pre-installed programs.

 

 

 

 

Agilent 490 System

The Agilent 490 Micro GC is a rugged, compact, laboratory quality gas chromatograph that delivers information you need, wherever you need it. The fifth generation 490 Micro GC is designed to provide maximum flexibility and ease-of use. You can customize with options including column modules and optimized sample conditioning to achieve greater sensitivity and performance. Your 490 Micro GC arrives pre-configured, factory tested for your analysis and ready to go. If your needs change, you can reconfigure in the field for new applications in just minutes with our user installable plug and play GC channels. The small size and weight of the 490 Micro GC, make it easy to carry between analysis sites in the field, such as perimeter monitoring, multiple drilling locations, and at natural gas pipelines and metering stations.

 

 

 

 

FIXED BED REACTOR

The reactor was design to perform pyrolysis and gasification in a bench-scale process. It is connected to the micro-GC to provide real time analysis of gases produced from the reactor as well as equipped with fluid-gas separator to collect fluid product such as bio-oil.

 

 

 

 

 

 

 

ULTRASONIC BATH CLEANER

Branson ultrasonic bath cleaners have 40kHz, industrial type transducers, coupled with sweep frequency capability, allowing you to get the best cleaning throughout the tank. The heated units have a temperature sensor that causes the heater to be shut off if the temperature exceeds 70 deg. C. The digital unit allows for easy display of all parameters. The 1/2 gal and 3/4 gal units feature convenient built-in pour drains while the larger models incorporate side tank drains with shut-off valve.

 

 

 

FURNACES

Carbolite Horizontal Tube Furnaces

    • Maximum operating temperature of 1200°C.
    • Designed to accept process tubes up to 6.5 inch OD.
    • Six different heated lengths of 18, 24, 30, 36, 42 and 48 inch provide for multiple working and uniformity requirements.
    • Insulating end vestibules improve chamber uniformity and incorporate interchangeable tube adapters.
    • These tube adapters allow convenient conversion to different diameter process tubes.
    • Long-life free radiating heating element design provides excellent radial and linear chamber uniformity.
    • High efficiency low mass vacuum formed ceramic fiber insulation enhances heat-up rates.

     

     

    Ashing Furnace - Lindberg Blue M 

    This Furnaces feature the latest technical advances in heating elements, insulation and temperature control, all integrated into a self-contained cabinet. The patented LGO heating element (light gauge overbend) delivers maximum radiant heat energy to the process load. The LGO element is partially imbedded within the exclusive Moldatherm® insulation, combined with unique double shell construction to provide optimum temperature uniformity, energy efficiency, fast response, quick heat-up and rapid cool-down.

     

     

     

     

     

    FLUID BATH

    Sub-Critical Water System

    These baths are ideal for subcritical water applications with a wide variety of temperature control requirements up to 200C (Oil Bath - Cole Parmer) and up to 400C (SS Salt Bath).

    Industrial-grade circulating pumps deliver extra pressure providing more efficient heat exchange, better temperature uniformity, and improved reservoir agitation. Long-life, highwattage heaters for applications requiring rapid temperature recovery from fluctuations.

     

     

     

     

     

     

    CENTRIFUGE

    Centrifuge Eppendorf 5702 

    The economical centrifuge for the clinical lab. With various fixed-angle and swing-bucket rotors and an extensive range of adapters, nearly all types of tubes can be used.

    All 5702 models can be used in a range of settings, from the clinical lab to the cell culture lab. With various fixed-angle and swing-bucket rotors available, they can accommodate almost any kind of tube.

     

     

     

     

     

     

     

    KARL-FISCHER TITRATOR

    870 Titrino plus 

    The Titrino plus is Metrohm's new Karl Fischer titrator for volumetric water determinations. It will measure water content from a few ppm up to 100% reliably and accurately in solid, liquid and gaseous samples. An easy-to-use interface makes this a perfect option for routine users. New monitoring features ensure that the system is always operating safely and accurately.

     

     

     

     

     

     

    MATERIAL HANDLING

    The Caleva Multi Lab (CML) 

    The Caleva Multi Lab (CML) incorporates a granulator, extruder and spheronizer within an "all-in-one" compact and robust unit. Not only can it save valuable laboratory bench space, but it has the capacity of demonstrating process efficiency by operating with batches between 10-100 g which is invaluable when working with rare and costly materials often used in product development trials.

     

     

     

     

     

     

    Pelletizer (Carver Auto Tablet Press, Model 3887)

    The benchtop Carver pelletizer Carver pellet presses are designed to compact homogeneous powder into a usable pellet sample. It is used in quality control and research and development to test sample preparations and destructive testings. Pellet dies are constructed of 440 stainless steel for corrosion resistance and include a pellet ejector.

     

     

     

     

     

     

     

    High Pressure/High Temperature Fixed Bed Reactor

    The high pressure fixed bed reactor is designed to perform CH4 conversion studies using different catalytic systems. It is connected to an online gas analyzer as well as a fluid-gas separator. The reactor is fully automated and equipped with various Mass Flow Controllers for different gas mixtures.

    STA 6000

    STA 6000
    TGA
    Micrometer
    Element Analyzer
    TGA Analyzer (TG-209 F1 Libra)
    TGA 8000
    ChemBET
    GAS CHROMATOGRAPHY
    HP 6890 GC-MS
    Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES)
    Microwave Synthesis/Digestion System (Multiwave 5000)
    Agilent 490 System
    FIXED BED REACTOR
    Bransonic Ultrasonic Cleaner - Branson 3510
    Furnace
    Ashing Furnace - Lindberg Blue M
    FLUID BATH
    CENTRIFUGE
    870 Titrino plus
    The Caleva Multi Lab (CML)
    Pelletizer (Carver Auto Tablet Press, Model 3887)
    High Pressure/High Temperature Fixed Bed Reactor